DIN 51075-2-1984 陶瓷材料的检验.碳化硅的化学分析.游离碳含量的直接测定
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【英文标准名称】:Testingofceramicmaterials;chemicalanalysisofsiliconcarbide;directdeterminationofthefreecarboncontent
【原文标准名称】:陶瓷材料的检验.碳化硅的化学分析.游离碳含量的直接测定
【标准号】:DIN51075-2-1984
【标准状态】:作废
【国别】:德国
【发布日期】:1984-03
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:分析;材料;碳;碳化硅;硅无机化合物;原材料;陶瓷;试验;含量测定;化学分析和试验
【英文主题词】:Analysis;Carbon;Ceramics;Chemicalanalysisandtesting;Determinationofcontent;Materials;Rawmaterials;Siliconcarbide;Siliconinorganiccompounds;Testing
【摘要】:Testingofceramicmaterials;chemicalanalysisofsiliconcarbide;directdeter-minationofthefreecarboncontentEssaidesmatièrescéramiques;analysechimiqueducarburedesilicium;déter-minationdirectedelateneurencarboneélémentaireIndies
【中国标准分类号】:Q30;G10
【国际标准分类号】:81_060_10
【页数】:7P;A4
【正文语种】:德语
【英文标准名称】:StandardTestMethodforDeterminationofPhenolicAntioxidantsandErucamideSlipAdditivesinPolypropyleneHomopolymerFormulationsUsingLiquidChromatography(LC)
【原文标准名称】:用液相色谱法对聚丙烯均聚物配方中酚醛抗氧化剂和酰胺纤维润滑添加剂测定的标准试验方法
【标准号】:ASTMD6042-2004
【标准状态】:作废
【国别】:
【发布日期】:2004
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D20.70
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:有机化合物;化工技术;液相色谱法;化学分析和试验;试验
【英文主题词】:additive;antioxidants;erucamideslip;extraction;Irgafos168;Irganox1010;Irganox1076;Irganox3114;liquidchromatography(LC);polypropylene(PP);vitaminE
【摘要】:Separationandidentificationofstabilizersusedinthemanufactureofpolypropyleneisnecessaryinordertocorrelateperformancepropertieswithpolymercomposition.Thistestmethodprovidesameanstodetermineerucamideslip,VitaminE,Irgafos168,Irganox3114,Irganox1010,andIrganox1076levelsinpolypropylenesamples.Thistestmethodisalsoapplicableforthedeterminationofotherantioxidants,suchasUltranox626,Ethanox330,SantanoxR,andBHT,buttheapplicabilityofthistestmethodhasnotbeeninvestigatedfortheseantioxidants.Theadditive-extractionprocedureismadeeffectivebytheinsolubilityofthepolymersampleinsolventsgenerallyusedforliquidchromatographicanalysis.Underoptimumconditions,thelowestlevelofdetectionforaphenolicantioxidantisapproximately2ppm.Note28212;Othermethodsthathavebeenusedsuccessfullytoremoveadditivesfromtheplasticsmatrixincludethinfilm,microwave,ultrasonic,andsupercriticalfluidextractions.OthermethodshavebeenusedsuccessfullytoseparateadditivesincludingSFCandcapillaryGC.Irgafos168isaphosphiteantioxidant.Phosphitesareknowntoundergobothoxidationandhydrolysisreactions.LessIrgafos168maybeseeninthepolymerthanoriginallyaddedtothepolymerduetooxidationduringprocessing.TheHPLCseparationiscapableofseparatingthephosphite,phosphate(oxidationproduct),andhydrolysisproductandquantifythemifstandardsareobtained.Nosignificantbreakdownofthephosphiteantioxidanthasbeenseenduetoeitherextractiontechniqueortheseparationpresentedinthisstandard.1.1Thistestmethodcoversaliquid-chromatographicprocedurefortheseparationofsomeadditivescurrentlyusedinpolypropylene.Theseadditivesareextractedwithacyclohexane:methylenechloridemixtureusingeitherrefluxorultrasonicbathpriortoliquid-chromatographicseparation.Theultravioletabsorbence(200nm)ofthecompound(s)ismeasured,andquantitationisperformedusingtheinternalstandardmethod.1.2Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.SpecificprecautionarystatementsaregiveninSection9.Note1-ThereisnosimilarorequivalentISOstandard.
【中国标准分类号】:G17
【国际标准分类号】:71_040_50;83_080_20
【页数】:5P.;A4
【正文语种】:
基本信息
标准名称: | 化工企业标准体系(原ZB/T G01 004-1990) |
中标分类: |
化工 >>
化工综合 >>
技术管理 |
发布日期: | 1990-04-01 |
实施日期: | 1991-01-01 |
首发日期: | 1900-01-01 |
作废日期: | 1900-01-01 |
出版日期: | 1900-01-01 |
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所属分类: 化工 化工综合 技术管理